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Author affiliations 1 Center for Integrated Nanotechnologies, Los Alamos National Laboratory, United States of America 2 Actinide Materials Processing & Power Division, Los Alamos National Laboratory, United States of America 3 Chemistry Division, Los Alamos National Laboratory, United States of America 4 National Security Education Center, Los Alamos National Laboratory, United States of America 5 Detonator Production Agency, Los Alamos National Laboratory, United States of America 6 Both authors equally contributed to this work. We present a methodology for developing ultra-thin and strong formvar-based membranes with controlled morphologies. Formvar is a thin hydrophilic and oleophilic polymer inert to most chemicals and resistant to radiation. The formvar-based membranes are viable materials as support structures in micro- and macro-scale systems depending on thinness and porosity control. Tunable sub-micron thick porous membranes with 20%–65% porosity were synthesized by controlling the ratios of formvar, glycerol, and chloroform. This synthesis process does not require complex separation or handling methods and allows for the production of strong, thin, and porous formvar-based membranes.
An expansive array of these membrane characterizations including chemical compatibility, mechanical responses, wettability, as well as the mathematical simulations as a function of porosity has been presented. The wide range of chemical compatibility allows for membrane applications in various environments, where other polymers would not be suitable.
Bappa Morya Re Pralhad Shinde Mp3 Song Free Download. Our formvar-based membranes were found to have an elastic modulus of 7.8 GPa, a surface free energy of 50 mN m −1 and an average thickness of 125 nm. Stochastic model simulations indicate that formvar with the porosity of ~50% is the optimal membrane formulation, allowing the most material transfer across the membrane while also withstanding the highest simulated pressure loadings before tearing. Development of novel, autodesk 3ds max 2012 crack xforce and versatile membranes with controlled porosity offers a wide range of exciting applications in the fields of nanoscience, microfluidics, and MEMS. Export citation and abstract. Formvar has been widely used as both a support material for various nano- and micro-structures in applications such as transmission electron microscopy (TEM) grids and microfluidic systems [, ].
The formvar molecular structure or Poly(vinyl) formal (CAS# 9003-33-2) reported by Sigma-Aldrich is shown to be [C 3H 6O 2] n with a reported density of 1.23 g ml −1. This polymer was found to be structurally stable at thickness of 50 nm, hydrophilic and oleophilic, inert to most acids and solvents, and can be made into porous structures . Additionally, formvar was found to have exceptional radiation tolerance and possesses interesting chemical, thermal and electrical properties [–].
Microfiltration is a process based around the osmotic pressure differential of two fluids wetting to and separated by a filter. The pore size in microfiltration membranes can range from ~0.05 to 10 μm . An example of this functionality is seen in recent efforts to use semipermeable membranes to desalinate water in a lab-on-a-chip system . Many of the current commercial systems use two relatively thick PTFE membranes one treated to be hydrophilic the other treated to be hydrophobic with 0.2 μm pore size.
Other membranes in such devices often face the challenge of remaining structurally stable under high fluid pressures . An ultra-strong and thin formvar membrane overcomes many of these challenges providing an adaptable support structure for thin filters in similar applications. Its flexible morphology also allows it to be transferred/placed onto a wide range of substrates including glass and ETFE. Formvar-based membranes can be used to enhance a range of systems beyond microfluidic applications. Thin membranes provide a way to increase the size and scalability of current pressure sensing systems that utilize 2D materials .